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doi: 10.1111/j.1469-8137.2009.03146.x

Samples must be collected within two to four hours post-administration to capture measurable concentrations, and immediate processing (centrifugation, plasma separation, freezing at 80C) is essential to prevent ex vivo degradation

Beck J, Miller D, Steinberg P, Andreeff M , Mertelsmann R, Koziner B, Good R, Gupta S